Full Automatic Parallel Micro High Pressure Reactor

Full Automatic Parallel Micro Reactor is used for chemistry and chemical engineering synthetic reaction under high temperature and high pressure or catalytic reaction, and such environmental conditions that needs to measure the pressure, temperature, and measuring speed at the same time, and add inert gas protection, pacify pressure and realize online-sampling or online feeding. And this instrument is integrated with America advanced technologies and China special patent design.

1. Volume: 25 ml, 50 ml, 100 ml, 200 ml, 500 ml for customized.

2. Body material: stainless steel 316L/pure titanium/hastalloy material (optional)

3. Working temperature: 250 ℃ / 450 ℃ (optional)

4. Working pressure: 10 MPa / 30 MPa (optional)

5. Valve and connection materials: SU316L stainless steel

6. Reactor liner: A grade PTFE or high-quality or liner, the liner has advantages of strong anti-corrosion, easy to disassemble and convenient to clean, etc.

7. Intelligent safety valve: 10MPA, 20MPA, 30MPA, decompression precision: 0.5PA.

8. Optical window material: adopted polishing JGS2 quartz glass (pressure-proof window) or sapphire mirror

9. Optical window diameter: 30 mm - 60 mm (optional)

10. Temperature-control heating device and uniform heat transfer design

11. Gas inlet function

12. Gas controls solenoid valve.

13. With circulating cooling solenoid valve to realize fast cooling. 

14. Online temperature and online pressure display

15. Strong magnetic stirring function under the bottom (users can choose our company’s overhead mechanical stirring method in case of high viscosity or large granular solid materials optionally).

16. There has auxiliary cooling or heating function in reactor.

17. With a high precision adjustable auto-decompression protection, the device achieved unique patent.

18. With the gas phase, liquid phase online detection connection pipe.

There are 2 stations,3 stations, 4 stations, 6 stations and 8 stations. The number of other stations can be customized.

1. It can display multi-digital high-voltage parallel temperature and pressure at the same time, and realize computer connection to perform PC control.

2. Each individual reactor has reflecting function of independent operation.

3. Each individual reactor has the over-pressure alarm and safety decompression function.

4. It can realize gas parallel or insert in ifunction of gas flow control.

5. Each reactor adopted patent type sealing design, which completely ensures good high-pressure sealing and corrosion resistance.

6. Synchronization and precision of heating speed and stirring speed are on all fours.  .

7. The observation window used the JGS2 quartz glass imported from Japan (only visible high voltage products).

8. It can realize to observe reaction conditions online under high pressure at the same time, and can also be used for light exposing and light catalytic reaction, even the ultraviolet light transmittance is over 95% (only visible high voltage products).

9. Each reactor can be implemented at the bottom of the magnetic stirring and magnetic coupling at the top of the machinery stirring.

Optional accessories: UV optical direct output unit, optical output unit, outer lens unit

u  Working temperature: pure titanium/ hartz alloy, the max. Temperature: 450℃; the material temperature of stainless steel is 250℃, the temperature precision is ±1℃. The standard configurations: a set of digital stirring device, pure titanium/316L/hartz alloy material reactor body(optional), oil bath heating/electric wire heating(optional), two needle valve, two ball valve, and one pressure gauge(digital pressure gauge is optional), a set of cooling coil, 1.5 meters stainless steel connection tube, online sampling tube, a set of TAIKANG special wrench.

u  Stirring speed and temperature are digitally displayed, rotary speed is 0-2000RPM, speed accuracy:±5RPM, power supply: 220V, 50Hz, stirring power: 25W-100W with the model, the heating power: 300W-1000W with the standard model. Insulating layer: adopted the aluminum silicate wool vacuum customized environmental heating preservation; insulation layer: use alkali-free glass fiber; insulation coefficient≥500 omen when the relative humidity is less than 35%. Working time: work for 96 hours continuously in a single.

u  Dial pressure value:25Mpa, and the minimum reading is 1pa. The minimum reading of digital pressure is 0.01 pa.

u  Valve pipes fit for the European standards, and the connectors all are the standard configuration. Ball valve can be connected with the inert gas bottle to carry out inert protection experiments, realize that reactants are not direct contact with air.

1. open the packaging, take out the kettle body and heating mixer first, add the reaction mass into the kettle, then tighten it and put into the heater (note: firstly connect the gas bottle with kettle body ball valve well before do the inert gas hydrogenation reaction ). Check the needle valve and ball valve in the closed circuit state, the power supply is 220V, and then turn on the switch to work.

2. adjust "stir" knob clockwise, and adjust it to a suitable location according to rotational speed display. Such as the large capacity or viscous solution in stirring, users can adjust knob to enhance stirring intensity.

3. temperature setting: press set key to heat, or press the set key  to reduce temperature, will quickly set out the required heating temperature, such as: 100 ℃, green light is bright than means heating, green light goes out means that the heating stops, the microcomputer confirm the heating quantity based on the setting temperature difference size of current temperature, and ensure the heating up for once without warm-stamping, and keep the heat balance of set value and display value under ±2.5 ℃ temperature differences, make the heating process more easily.

4. self-adjusting function: start the self-adjusting function, when there is no any disciplines between the different heating stage or heating power with solution, the heating time will shorten, blunt temperature and balance are best, but self-adjusting should be reset after changing the heating medium or heating conditions.

5. start self-adjusting: press the shift key 5 seconds, the number in setting window flashes, and it means to enter into self-adjusting state, stop the number stop flashing after three warm-stamping, and it means self-adjusting stopped, users can use it, but self-adjusting needs to be used in the initial heating, and the self-adjusting is uncertainty on halfway.

6. There has a rubber plug behind stirrer to protect the topical thermocouple socket avoiding the rust and corrosion for use, unplug it and the inside probe disconnected, the machine stopped working. If when using a topical thermocouple, the plug should be preserved out, and insert the plug of topical thermocouple into socket and lock nut, and then put the stainless steel rods into the solution for temperature control of heating.

7. the instrument is equipped with power protection function, when the thermocouple connection is bad,  hundred-bit values of display Windows is 1 or HHHH, the green light goes out, instruments stop heating automatically, reuse it after installation shall be checked in good condition.

1. please connect ground wire well in order to ensure the safe use, please do not operate without material or dry burning.

2. In order to extend the use of the product, the motor of magnetic stirrer has the fan cooling function, so the instrument can’t be used for heating individually when doing heating experiment especially the high-temperature heating experiments; do not adjust the motor to rotate or medium speed rotating state (or idle), in case of the motor and instrument is damaged by heat radiation.

3. at the end of the high temperature heating, please turn off the heating switch, stay a few minutes after remaining warming dispersed, and then turn off stirring switch. The temperature of heating section is higher, be careful in work to prevent burns.

4. The new instrument is used for the first time, there has white smoke and peculiar smell in cover where adopted the heating wire for heating, and it is normal phenomenon that the white smoke is emitted color from white to brown and then again became white, because the glass fiber contains oil and other compounds in the process of production, thus the glass fiber should be put in ventilated place, it can be used normally after disappear in a few minutes.

5. The liquid enter into cover, please shut off the power, put the instrument in ventilated place to stay dry and in order to avoid leakage risk or electric short circuit occurred.

6. when the environment relative humidity is too large, there may be a induced electricity go  through the insulation layer to the shell, please be sure to connect ground wire to avoid leakage and pay attention to ventilation. Relative humidity ranges: 35%-85% (without condensation)

7. Please put the instrument in the dry and no corrosive environment for preserving if the instrument is not used in a long time.

8. If there has any differences between the product and the instruction due to the improvement of the content, please forgive no further notice, please call for details to the manufacturer.

Packing and Shipping
-The main parts will be wrapped with foam,then put into the carton; the mainbody portion will be packed in wooden cases;
-Both neutral and customized packaging can be available.

-We can ship the goods to you by International Express such as DHL,UPS,TNT,EMS and so on, you can also choose the appropriate one based on your timeline and budget. Besides,you can choose to use your own shipping agent